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<title>Baseline Evaluation of XAFS Bending Magnet Beamlines</title>
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<p class=MsoNormal style='text-align:justify;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>Baseline Evaluation
of XAFS Bending Magnet Beamlines<o:p></o:p></span></p>
<p class=MsoNormal style='text-align:justify;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>Experiments performed
under “<i style='mso-bidi-font-style:normal'>standard optimized operating
conditions</i>,” as recorded.<o:p></o:p></span></p>
<div class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<table class=MsoNormalTable border=0 cellspacing=0 cellpadding=0
style='margin-left:5.4pt;border-collapse:collapse;mso-padding-alt:0in 5.4pt 0in 5.4pt'>
<tr style='mso-yfti-irow:0;height:15.9pt'>
<td width=150 valign=top style='width:112.5pt;padding:0in 5.4pt 0in 5.4pt;
height:15.9pt'>
<p class=MsoBodyText style='line-height:150%'><span style='font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>Trudy Bolin</span><span
style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1;height:15.95pt'>
<td width=150 valign=top style='width:112.5pt;padding:0in 5.4pt 0in 5.4pt;
height:15.95pt'>
<p class=MsoBodyText style='line-height:150%'><span style='font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>Steve Heald</span><span
style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2;height:15.95pt'>
<td width=150 valign=top style='width:112.5pt;padding:0in 5.4pt 0in 5.4pt;
height:15.95pt'>
<p class=MsoBodyText style='line-height:150%'><span style='font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>Matt Newville</span><span
style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:3;mso-yfti-lastrow:yes;height:15.95pt'>
<td width=150 valign=top style='width:112.5pt;padding:0in 5.4pt 0in 5.4pt;
height:15.95pt'>
<p class=MsoBodyText style='line-height:150%'><span style='font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>Julie Cross</span><span
style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
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<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Rh coated torroidal focusing mirror after the monochromator. Secondary
Rh coated flat mirror for harmonic rejection.<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Detectors: Custom 10 cm gas ionization chambers operated at 300
VDC with He, ca. 400 VDC with other gases (nitrogen).<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Beamline optimized for low energies (e.g., sulfur K), so detectors
run windowless and effectively serve as part of the flight path. Changing
samples requires re-equillibration time of ca. 1 minute. <o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>XAFS scanning is done using spec. Software automatically measures
offsets for 10 seconds at the start of every scan.<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Monochromator Si(111) double flat crystals in fixed-exit geometry.<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>SRS 570 current amplifiers > V/F converter from Nova > VME
Scaler<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Vertical feedback uses PSD on torroidal mirror pitch. Horizontal
feedback uses PSD on monochromator 2<sup>nd</sup> crystal chi.<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>7 GeV electron synchrotron operating in Non top-up mode, 0 +
1296x1, 1% coupling, 98.7 mA at 11:43 am.<o:p></o:p></span></p>
<p class=MsoNormal style='margin-left:.25in;text-align:justify;text-indent:
-.25in;line-height:150%;mso-list:l0 level1 lfo4;tab-stops:list .25in'><![if !supportLists]><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
"Courier New";mso-fareast-font-family:"Courier New";color:black'><span
style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Beam size at sample position varies, but depends on torroidal
focusing mirror settings.<o:p></o:p></span></p>
<p class=MsoNormal style='text-align:justify;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p> </o:p></span></p>
<span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-fareast-font-family:"Times New Roman";mso-bidi-font-family:
"Times New Roman";color:black;mso-ansi-language:EN-US;mso-fareast-language:
EN-US;mso-bidi-language:AR-SA'><br clear=all style='page-break-before:always'>
</span>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>ENERGY CALIBRATION: Experiment log<o:p></o:p></span></p>
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style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoBodyText style='line-height:150%'><span style='font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>XANES scans of metal foil
reference standards collected over a large energy range without recalibrating
the monochromator. <o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l2 level1 lfo5;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Metal foils from EXAFS Materials (Joe Wong’s
company). Set provided by M. Newville.<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l2 level1 lfo5;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>XANES scan: -20 to 30 eV, step sizes as noted in
table <o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l2 level1 lfo5;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Switch to N2 in IT for Cu and Zn measurements.<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="37%" rowspan=2 valign=top style='width:37.3%;border:solid windowtext 1.0pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>file name</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="6%" rowspan=2 valign=top style='width:6.22%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>foil</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="41%" colspan=2 valign=top style='width:41.56%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>edge
energy</span><span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;
line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p></o:p></span></p>
</td>
<td width="14%" rowspan=2 valign=top style='width:14.92%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid blue .5pt;mso-border-alt:solid windowtext .5pt;
mso-border-left-alt:solid blue .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>step size (eV)</span><span style='font-size:
10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>nominal†</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>measured‡</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2;height:11.4pt'>
<td width="37%" valign=top style='width:37.3%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.4pt'>
<p class=MsoNormal style='line-height:150%;tab-stops:right 93.85pt'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>copper_foil_XANES_Apr21_2006_1515.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="6%" valign=top style='width:6.22%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Cu</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>8980.48(2)</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>8984.22</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="14%" valign=top style='width:14.92%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
mso-border-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.4</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:3;height:11.45pt'>
<td width="37%" valign=top style='width:37.3%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>zinc_foil_XANES_Apr21_2006_1528.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="6%" valign=top style='width:6.22%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Zn</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>9660.76(3)</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>9665.07</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="14%" valign=top style='width:14.92%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
mso-border-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.4</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:4;height:11.45pt'>
<td width="100%" colspan=5 valign=top style='width:100.0%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>changed 2</span><sup><span style='font-size:
10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>nd</span></sup><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'> mirror
tilt so cutoff is ca. 12keV (tilt is measured relative to torroidal mirror
tilt). Detectors at 1 kV,</span><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Detector gases changed to nitrogen.</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:5;mso-yfti-lastrow:yes;height:11.45pt'>
<td width="37%" valign=top style='width:37.3%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>zinc_foil_XANES_Apr21_2006_1606.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="6%" valign=top style='width:6.22%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Zn</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>9660.76(3)</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" valign=top style='width:20.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>9665.36</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="14%" valign=top style='width:14.92%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
mso-border-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.4</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
</table>
<p class=MsoNormal style='text-align:justify;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='text-align:justify;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>He in IT for Cr and V
measurements.<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="42%" rowspan=2 valign=top style='width:42.4%;border:solid windowtext 1.0pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>file name</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" rowspan=2 valign=top style='width:10.48%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>foil</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="31%" colspan=2 valign=top style='width:31.86%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>edge
energy</span><span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;
line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p></o:p></span></p>
</td>
<td width="15%" rowspan=2 valign=top style='width:15.26%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid blue .5pt;mso-border-alt:solid windowtext .5pt;
mso-border-left-alt:solid blue .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>step size (eV)</span><span style='font-size:
10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="12%" valign=top style='width:12.56%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>nominal†</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="19%" valign=top style='width:19.28%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>measured‡</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2;height:11.45pt'>
<td width="42%" valign=top style='width:42.4%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>chromium_foil_xanes_apr21_2006_1356.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Cr</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="12%" valign=top style='width:12.56%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>5989.02(4)</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="19%" valign=top style='width:19.28%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>5990.43</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="15%" valign=top style='width:15.26%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
mso-border-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.3</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:3;height:11.45pt'>
<td width="42%" valign=top style='width:42.4%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>vanadium_foil_xanes_apr21_2006_1259.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>V (5µm) </span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="12%" valign=top style='width:12.56%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>5463.76(5)</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="19%" valign=top style='width:19.28%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><5465> calibrated</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="15%" valign=top style='width:15.26%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
mso-border-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.3</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:4;mso-yfti-lastrow:yes;height:11.45pt'>
<td width="42%" valign=top style='width:42.4%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>vanadium_foil_xanes_apr21_2001_1313.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>V</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="12%" valign=top style='width:12.56%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>5463.76(5)</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="19%" valign=top style='width:19.28%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>5464.72</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="15%" valign=top style='width:15.26%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
mso-border-alt:solid windowtext .5pt;mso-border-left-alt:solid blue .5pt;
padding:0in 5.4pt 0in 5.4pt;height:11.45pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.3</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
</table>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:blue'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>N.B. Mo, Ag and Cd not accessible<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>†Rev. Sci. Instrum., <b style='mso-bidi-font-weight:
normal'>67</b> (1996) 686.<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>‡Using first peak in first derivative of XANES
calculated at beamline with CMC-CAT regional software (Xplot).<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>ENERGY RESOLUTION: Experiment log<o:p></o:p></span></p>
<div class=MsoBodyText align=center style='text-align:center;line-height:150%'><span
style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoBodyText style='line-height:150%'><span style='font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'>Measure the full width at
half maximum of the V<sub>2</sub>O<sub>5</sub> pre-edge feature. <o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l4 level1 lfo6;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>The sample is powder-on-tape prepared by Matt
Newville. <o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l4 level1 lfo6;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Scan details:<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>–100, -20, 5eV steps<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>–20, 30, 0.2 eV steps<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>2.81, 8, 0.075 Å<sup>-1</sup> steps<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.5 s/pt (w/1 s/pt settling time)<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="36%" rowspan=2 valign=top style='width:36.12%;border:solid windowtext 1.0pt;
border-right:solid black 1.0pt;mso-border-alt:solid windowtext .5pt;
mso-border-right-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>filename</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="20%" colspan=2 valign=top style='width:20.12%;border:solid black 1.0pt;
border-left:none;mso-border-left-alt:solid black .5pt;mso-border-alt:solid black .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>beam
size (focused)</span><span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;
line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p></o:p></span></p>
</td>
<td width="43%" rowspan=2 valign=top style='width:43.76%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Notes</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="10%" valign=top style='width:10.06%;border-top:none;border-left:
none;border-bottom:solid black 1.0pt;border-right:solid black 1.0pt;
mso-border-top-alt:solid black .5pt;mso-border-left-alt:solid black .5pt;
mso-border-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>V</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.06%;border-top:none;border-left:
none;border-bottom:solid black 1.0pt;border-right:solid black 1.0pt;
mso-border-top-alt:solid black .5pt;mso-border-left-alt:solid black .5pt;
mso-border-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>H</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2'>
<td width="36%" valign=top style='width:36.12%;border-top:none;border-left:
solid windowtext 1.0pt;border-bottom:solid windowtext 1.0pt;border-right:
solid black 1.0pt;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;mso-border-right-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%;tab-stops:right 120.05pt'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>vanadate_EXAFS_Apr21_2006_1325.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.06%;border-top:none;border-left:
none;border-bottom:solid black 1.0pt;border-right:solid black 1.0pt;
mso-border-top-alt:solid black .5pt;mso-border-left-alt:solid black .5pt;
mso-border-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>ca. 1 mm</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.06%;border-top:none;border-left:
none;border-bottom:solid black 1.0pt;border-right:solid black 1.0pt;
mso-border-top-alt:solid black .5pt;mso-border-left-alt:solid black .5pt;
mso-border-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>ca. 1 mm</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="43%" valign=top style='width:43.76%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Aborted; sample chamber gas not at equilibrium
</span><span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:
150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:3;mso-yfti-lastrow:yes'>
<td width="36%" valign=top style='width:36.12%;border-top:none;border-left:
solid windowtext 1.0pt;border-bottom:solid windowtext 1.0pt;border-right:
solid black 1.0pt;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;mso-border-right-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%;tab-stops:right 120.05pt'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>vanadate_EXAFS_Apr21_2006_1331.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.06%;border-top:none;border-left:
none;border-bottom:solid black 1.0pt;border-right:solid black 1.0pt;
mso-border-top-alt:solid black .5pt;mso-border-left-alt:solid black .5pt;
mso-border-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>“</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.06%;border-top:none;border-left:
none;border-bottom:solid black 1.0pt;border-right:solid black 1.0pt;
mso-border-top-alt:solid black .5pt;mso-border-left-alt:solid black .5pt;
mso-border-alt:solid black .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>“</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="43%" valign=top style='width:43.76%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
</td>
</tr>
</table>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>FLUX: Experiment log<o:p></o:p></span></p>
<div class=MsoBodyText align=center style='text-align:center;line-height:150%'><span
style='font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Monochromator set to 10 keV<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Nitrogen flowing at STP<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>1,000 VDC across detector plates<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Incident beam focused by torroidal mirror to ca. 1 mm V x 1 mm H<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>10 cm ADC gas ionization chamber (GSECARS)<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Unsure of v/f conversion factor. Can probably figure that out from
these number:<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>ring current = 98.8 mA, scaler output is 472560 counts/sec<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>centering beam on IT using a table scan (slow). Discover that the
Zn foil is still in the beam. Oops.<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Output voltage: 20 nA/V<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Offset voltage: 1 pA<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>V-F conversion factor<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Scaler counts 11770 – 280<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>For comparison, in I0 10 cm, 1kV, 10 keV, Nitrogen, <o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>Scaler counts 149056 – 1<o:p></o:p></span></p>
<p class=MsoNormal style='text-indent:.5in'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'>gaoin settings are 20 nA/V, 1pA offset.<o:p></o:p></span></p>
<p class=MsoNormal><span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>BASE NOISE LEVEL: Experiment Log<o:p></o:p></span></p>
<div class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Record at 10 keV for 3 minutes. Record with beam
off for 3 minutes.<span style='mso-spacerun:yes'> </span>Record data with
knife edge 1/2 way through beam, Horizontal and Vertical, for 3 minutes. Set
delay time to 0 seconds.<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="38%" valign=top style='width:38.08%;border:solid windowtext 1.0pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>filename</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="35%" valign=top style='width:35.44%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>condition</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="26%" valign=top style='width:26.48%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>notes</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="38%" valign=top style='width:38.08%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>timescan.dat #S 1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="35%" valign=top style='width:35.44%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>10 keV</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="26%" valign=top style='width:26.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2'>
<td width="38%" valign=top style='width:38.08%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>timescan.dat #S 2</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="35%" valign=top style='width:35.44%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>beam off</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="26%" valign=top style='width:26.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:3;mso-yfti-lastrow:yes'>
<td width="38%" valign=top style='width:38.08%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>timescan.dat #S 3</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="35%" valign=top style='width:35.44%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>1/2 blocked vertically</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="26%" valign=top style='width:26.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>using slit, from bottom</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
</table>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>DETECTOR LINEARITY: Experiment Log<o:p></o:p></span></p>
<div class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Slit scan: scan a narrow slit across the beam
horizontally, to see how uniform the detector is from side to side.<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="18%" rowspan=2 valign=top style='width:18.86%;border:solid windowtext 1.0pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>filename</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="21%" colspan=2 valign=top style='width:21.56%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>beam size</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="8%" rowspan=2 valign=top style='width:8.48%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>IO</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="8%" rowspan=2 valign=top style='width:8.48%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>IT</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="42%" rowspan=2 valign=top style='width:42.62%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>comments</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="10%" valign=top style='width:10.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>H</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>V</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2;mso-yfti-lastrow:yes'>
<td width="18%" valign=top style='width:18.86%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>timescan.dat S# 5</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>ca. 1 mm</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.78%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>ca. 1 mm</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="8%" valign=top style='width:8.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>2 nA/V</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="8%" valign=top style='width:8.48%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>2 nA/V</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="42%" valign=top style='width:42.62%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>check uniformity of the ionization chambers </span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>from side to side</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>using a 0.1 mm wide slit</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
</table>
<p class=MsoNormal style='line-height:150%'><u><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p><span style='text-decoration:none'> </span></o:p></span></u></p>
<span style='font-size:10.0pt;mso-bidi-font-size:12.0pt;font-family:Arial;
mso-fareast-font-family:"Times New Roman";mso-bidi-font-family:"Times New Roman";
color:black;mso-ansi-language:EN-US;mso-fareast-language:EN-US;mso-bidi-language:
AR-SA'><br clear=all style='page-break-before:always'>
</span>
<p class=MsoBodyText2>HARMONIC CONTENT: Experiment log</p>
<div class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Scan the energy around 6.66 keV through a Mo
foil to look for emergent Mo XANES from the third harmonic. Scan parameters are
the same as for the Vanadate, but with larger steps in the XANES region.<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l1 level1 lfo7;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Nominal edge position for Mo is 20,000 eV. Run a
XANES scan with E0 = 6,667. <o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l1 level1 lfo7;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>25 µm thick Mo foil from sector 20.<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.25in;text-indent:-.25in;line-height:
150%;mso-list:l4 level1 lfo6;tab-stops:list .25in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Scan details:<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>–100, -20, 5 eV steps<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>–20, 30, 2 eV steps<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>2.81, 8, 0.075 Å<sup>-1</sup> steps<o:p></o:p></span></p>
<p class=MsoBodyText style='margin-left:.75in;text-indent:-.25in;line-height:
150%;mso-list:l4 level2 lfo6;tab-stops:list .75in'><![if !supportLists]><span
style='font-family:"Courier New";mso-fareast-font-family:"Courier New";
color:black'><span style='mso-list:Ignore'>o<span style='font:7.0pt "Times New Roman"'>
</span></span></span><![endif]><span style='font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>0.5 s/pt (w/1 s/pt settling time)<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="36%" valign=top style='width:36.66%;border:solid windowtext 1.0pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>filename</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="63%" valign=top style='width:63.34%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>notes</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="36%" valign=top style='width:36.66%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>moly_EXAFS_Apr21_2006_1426.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="63%" valign=top style='width:63.34%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>signal too low in IT; need to go to more
absorbing detector gas</span><span style='font-size:10.0pt;mso-bidi-font-size:
12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:"Times New Roman";
color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2;mso-yfti-lastrow:yes'>
<td width="36%" valign=top style='width:36.66%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>moly_EXAFS_Apr21_2006_1457.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="63%" valign=top style='width:63.34%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>with nitrogen in IT.</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
</table>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Changed over to nitrogen in IT. Starting at
14:53, with connecting a regulator to the gas bottle.<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>DATA QUALITY: Experiment log<o:p></o:p></span></p>
<div class=MsoNormal align=center style='text-align:center;line-height:150%'><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:
Arial;mso-bidi-font-family:"Times New Roman";color:black'>
<hr size=2 width="100%" align=center>
</span></div>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Transmission EXAFS of solutions with 0.1 edge
step in ca. 2 absorption lengths of water.<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>Solutions and transmission cells prepared by
Matt Newville using dilution calculations by Bruce Ravel.<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>zinc nitrate <o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>N.B. New solutions made. Need to update Matt’s
dilution notes for 12, 33 and 9 BM.<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:blue'>445 mg Zn(NO<sub>3</sub>)2•6H<sub>2</sub>O (Alfa
#22403)<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:blue'>was dissolved into ≈40 ml H<sub>2</sub>O
(Fischer W2-4 DIVF water) and stirred for 5 minutes.<o:p></o:p></span></p>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:blue'>The solution was then brought to 50 ml.<o:p></o:p></span></p>
<table class=MsoNormalTable border=1 cellspacing=0 cellpadding=0 width="100%"
style='width:100.0%;border-collapse:collapse;border:none;mso-border-alt:solid windowtext .5pt;
mso-padding-alt:0in 5.4pt 0in 5.4pt;mso-border-insideh:.5pt solid windowtext;
mso-border-insidev:.5pt solid windowtext'>
<tr style='mso-yfti-irow:0'>
<td width="42%" valign=top style='width:42.88%;border:solid windowtext 1.0pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>filename</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.04%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
</td>
<td width="18%" valign=top style='width:18.56%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>edge step height</span><span style='font-size:
10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;
mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="28%" valign=top style='width:28.52%;border:solid windowtext 1.0pt;
border-left:none;mso-border-left-alt:solid windowtext .5pt;mso-border-alt:
solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>notes</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:1'>
<td width="42%" valign=top style='width:42.88%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>zn_solution_EXAFS_Apr21_2006_1716.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.04%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>1 sec/pt</span><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="18%" valign=top style='width:18.56%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'><o:p> </o:p></span></p>
</td>
<td width="28%" valign=top style='width:28.52%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>XANES scan to check signal</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
</tr>
<tr style='mso-yfti-irow:2'>
<td width="42%" valign=top style='width:42.88%;border:solid windowtext 1.0pt;
border-top:none;mso-border-top-alt:solid windowtext .5pt;mso-border-alt:solid windowtext .5pt;
padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Arial;mso-bidi-font-family:
"Times New Roman";color:black'>zn_solution_EXAFS_Apr21_2006_1718.1</span><span
style='font-size:10.0pt;mso-bidi-font-size:12.0pt;line-height:150%;
font-family:Arial;mso-bidi-font-family:"Times New Roman";color:black'><o:p></o:p></span></p>
</td>
<td width="10%" valign=top style='width:10.04%;border-top:none;border-left:
none;border-bottom:solid windowtext 1.0pt;border-right:solid windowtext 1.0pt;
mso-border-top-alt:solid windowtext .5pt;mso-border-left-alt:solid windowtext .5pt;
mso-border-alt:solid windowtext .5pt;padding:0in 5.4pt 0in 5.4pt'>
<p class=MsoNormal style='line-height:150%'><span style='font-size:10.0pt;
mso-bidi-font-size:12.0pt;line-height:150%;font-family:Ar